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A Cation-Dependent Dual Activation Motif for Anionic Ring-Opening Polymerization of Cyclic Esters

https://doi.org/10.1021/jacs.2c01436

Jadrich, Caleb N. ; Pane, Vince E. ; Lin, Binhong ; Jones, Gavin O. ; Hedrick, James L. ; Park, Nathaniel H. ; Waymouth, Robert M. ( May 2022 , Journal of the American Chemical Society)

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Ultrafast and Controlled Ring-Opening Polymerization with Sterically Hindered Strong Bases

https://doi.org/10.1021/acs.macromol.0c01571

Lin, Binhong ; Jadrich, Caleb N. ; Pane, Vince E. ; Arrechea, Pedro L. ; Erdmann, Tim ; Dausse, Charles ; Hedrick, James L. ; Park, Nathaniel H. ; Waymouth, Robert M. ( October 2020 , Macromolecules)
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Nanocombinatorics with Cantilever-Free Scanning Probe Arrays

https://doi.org/10.1021/acsnano.8b08185

Brown, Keith A. ; Hedrick, James L. ; Eichelsdoerfer, Daniel J. ; Mirkin, Chad A. ( January 2019 , ACS Nano)

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Catalyst discovery through megalibraries of nanomaterials

https://doi.org/10.1073/pnas.1815358116

Kluender, Edward J. ; Hedrick, James L. ; Brown, Keith A. ; Rao, Rahul ; Meckes, Brian ; Du, Jingshan S. ; Moreau, Liane M. ; Maruyama, Benji ; Mirkin, Chad A. ( December 2018 , Proceedings of the National Academy of Sciences)

The nanomaterial landscape is so vast that a high-throughput combinatorial approach is required to understand structure–function relationships. To address this challenge, an approach for the synthesis and screening of megalibraries of unique nanoscale features (>10,000,000) with tailorable location, size, and composition has been developed. Polymer pen lithography, a parallel lithographic technique, is combined with an ink spray-coating method to create pen arrays, where each pen has a different but deliberately chosen quantity and composition of ink. With this technique, gradients of Au-Cu bimetallic nanoparticles have been synthesized and then screened for activity by in situ Raman spectroscopy with respect to single-walled carbon nanotube (SWNT) growth. Au₃Cu, a composition not previously known to catalyze SWNT growth, has been identified as the most active composition.

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Structural Evolution of Three-Component Nanoparticles in Polymer Nanoreactors

https://doi.org/10.1021/jacs.7b03163

Chen, Peng-Cheng ; Du, Jingshan S. ; Meckes, Brian ; Huang, Liliang ; Xie, Zhuang ; Hedrick, James L. ; Dravid, Vinayak P. ; Mirkin, Chad A. ( July 2017 , Journal of the American Chemical Society)